{"id":54,"date":"2020-11-18T18:31:21","date_gmt":"2020-11-18T21:31:21","guid":{"rendered":"https:\/\/lidmaexactasunlp.wordpress.com\/?page_id=54"},"modified":"2026-01-16T16:57:41","modified_gmt":"2026-01-16T19:57:41","slug":"publicaciones","status":"publish","type":"page","link":"https:\/\/lidma.exactas.unlp.edu.ar\/index.php\/publicaciones\/","title":{"rendered":"Publicaciones, Tesis y Tesinas"},"content":{"rendered":"\n

En nuestro laboratorio mantenemos y promovemos un fuerte compromiso con la investigaci\u00f3n y el desarrollo de metodolog\u00edas y tecnolog\u00edas de an\u00e1lisis espec\u00edficas para distintos tipos de muestras y matrices que mejoren el rendimiento de los m\u00e9todos anal\u00edticos vigentes, materializ\u00e1ndose en los numerosos trabajos cient\u00edficos publicados por los integrantes del laboratorio en revistas de alto impacto tanto a nivel nacional como internacional.<\/em><\/p>\n\n\n\n

PUBLICACIONES CIENT\u00cdFICAS<\/strong><\/p>\n\n\n\n

A\u00d1O 2025<\/strong><\/p>\n\n\n\n

“Multidimensional chromatography: A powerful technique in analysis of chiral agrochemicals in environment”
Sebastian J.\u00a0Caruso,\u00a0Agustin\u00a0Acquaviva,\u00a0Cecilia B.\u00a0Castells
Comprehensive Analytical Chemistry doi<\/a> – ISBN: 978-0-443-34581-4<\/p>\n\n\n\n

\u201cGas-liquid chromatography as a tool to determine vapor pressure of low-volatility pesticides: a critical study\u201d
Clara Parzanese, Carlina Lancioni, Cecilia Castells
Analytica Chimica Acta, 1354, 343932, 2025 doi<\/a> <\/p>\n\n\n\n

“Comprehensive antioxidant profiling and TAC determination in Stevia rebaudiana leaves using on-line HPLC\u2013CUPRAC: Evaluation of three different post-column derivatization reactor workflows”
Agust\u00edn\u00a0Acquaviva,\u00a0Arianne\u00a0Soliven,\u00a0Cecilia B.\u00a0Castells
Microchemical Journal doi<\/a><\/p>\n\n\n\n

\u201cSolid-Phase Microextraction\u201d
A. Buongarzoni; M. Tascon; C. Lancioni
Comprehensive Sampling and Sample Preparation, 2nd edition \u2013 doi<\/a> – ISBN: 9780124095472.<\/p>\n\n\n\n

“Development of solid-phase microextraction fibers based on hybrid MIL-68(Fe)@MIL101(Fe) for the analysis of polycyclic aromatic hydrocarbons in surface waters”
Sol Giovannoni, Gabriela A. Ortega-Moreno, Griselda Narda, Mario Reta, Carlina Lancioni
Microchemical Journal; 113143; 2025 doi<\/a> <\/p>\n\n\n\n

A\u00d1O 2024<\/strong><\/p>\n\n\n\n

“Enantiomeric purity determination of lactofen formulations through Chemometric Deconvolution of partially overlapped chromatographic profiles”
Mat\u00edas E. D\u00edaz\u00a0Merino,\u00a0Sof\u00eda R.\u00a0Peirano,\u00a0Roc\u00edo B.\u00a0Pellegrino Vidal,\u00a0Juan M.\u00a0Padr\u00f3,\u00a0Cecilia B.\u00a0Castells
Journal of Chromatography Open doi<\/a><\/p>\n\n\n\n

“Hybrid organic monolithic column containing MIL-68(Al) for the separation of small molecules by capillary HPLC.”
Sof\u00eca Raquel Peirano, Daiana Lorena Prince, Sol Giovannoni, Elisabeth Contreras Aguilar, Marcelo Ceol\u00edn, Matias Rafti, Sonia Keunchkarian, Romina Noel Echevarria, Mario Roberto Reta.
Journal of Chromatography A, 1733, (2024) 465258 doi<\/a><\/p>\n\n\n\n

“Modulation optimization when using a splitter pump after the first dimension in comprehensive two- dimensional liquid chromatography”
Agust\u00edn\u00a0Acquaviva,\u00a0Cecilia B.\u00a0Castells
Journal of Chromatography A doi<\/a><\/p>\n\n\n\n

“Optimization of resolution as a simultaneous function of solvent composition, pH and temperature in reversed-phase liquid chromatography”
Caruso, S.J., Cifuente, P.N., Castells, C.B., Gagliardi, L.G.
Analytica Chimica Acta, 1311, (2024) 342657 doi<\/a><\/p>\n\n\n\n

“Quality control of Bradyrhizobium inoculant strains: detection of nosZ and correlation of symbiotic efficiency with soybean leaf chlorophyll levels”
Dami\u00e1n Brignoli, Emilia Frickel-Critto, Tamara J. Sandobal, Roc\u00edo S. Balda, Cecilia B. Castells, El\u00edas J. Mongiardini, Julieta P\u00e9rez-Gim\u00e9nez, An\u00edbal R. Lodeiro
Front. Agron., (2024) Sec. Plant-Soil Interactions, doi<\/a><\/p>\n\n\n\n

“Simultaneous analysis of cannabinoids and terpenes in Cannabis sativa inflorescence using full comprehensive two-dimensional liquid chromatography coupled to smart active modulation”
Caruso, S.J., Acquaviva, A., M\u00fcller, J.L., Castells, C.B.
Journal of Chromatography A, 1720, (2024), 464810 doi<\/a><\/p>\n\n\n\n

“Enantiomeric purity determination of lactofen formulations through Chemometric Deconvolution of partially overlapped chromatographic profiles”
Mat\u00edas E. D\u00edaz Merino, Sof\u00eda R. Peirano, Roc\u00edo B. Pellegrino Vidal, Juan M. Padr\u00f3, Cecilia B. Castells.
Journal of Chromatography Open, 6, (2024), 100144 doi<\/a><\/p>\n\n\n\n

“New sorbents for sample pretreatment: development and applications”
Federico N. Casta\u00f1eda, Sofia R. Peyrano, Diana L. Prince, Sol Giovannoni, Romina N. Echevarria, Sonia Keunchkarian, Mario Reta
Trends in Analytical Chemistry, 180, (2024), 117924 doi<\/a><\/p>\n\n\n\n

“Aqueous Size Exclusion Chromatography applied to polymer analysis: experimental conditions and molecular weight calibration curves”
Rocio B. Pellegrino Vidal, Federico N. Casta\u00f1eda, Mariano E. Garrido, Juan M. Padr\u00f3
Journal of Chromatography A, 1729, (2024) doi<\/a><\/p>\n\n\n\n

“Validation and Regulatory Issues for Sample Preparation”
Autores: Federico N. Casta\u00f1eda, Sol Giovannoni, Sebastian J. Caruso, Juan M. Padr\u00f3
Comprehensive Sampling and Sample Preparation, 2da Edici\u00f3n, 2024 (ISBN 9780123813749), (2024) doi<\/a><\/p>\n\n\n\n

“Untargeted Chromatographic Methods Coupled with Chemometric Strategies for the Analysis of Food and Related Samples”
Federico N. Casta\u00f1eda, Rocio B. Pellegrino Vidal, Juan Aspromonte
Trends in Analytical Chemistry, 113, (2024) doi.<\/a><\/p>\n\n\n\n

\u201cEnantioseparation of pesticides by gas chromatography. Measurement of association constants enantiomer-chiral selector\u201d
Emilia Frickel Critto, Daiana Prince, Carlina Lancioni, <\/em>Cecilia Castells
Journal of Cromatography A, 465172; (2024) doi<\/a><\/p>\n\n\n\n

\u201cEnantioseparation of agrochemicals by gas chromatography.
Exploring columns based on cyclodextrin derivatives dissolved into polysiloxanes\u201d
Emilia Frickel Critto, Sol Giovannoni, Carlina Lancioni, Cecilia Castells
Journal of Separation Science, 47, 2300804; (2024) doi<\/a><\/p>\n\n\n\n

A\u00d1O 2023<\/strong><\/p>\n\n\n\n

\u201cDetermination of gas-polydimethylsiloxane distribution constants of
major Cannabis terpenes and terpenoids by capillary gas-liquid
chromatography\u201d.
Sol Giovannoni, Emilia Frickel Critto, Carlina Lancioni, Nicol\u00e1s Ronco,
Cecilia Castells
J. Chromatogr. A, 463998 (2023); doi<\/a>.<\/p>\n\n\n\n

\u201cDetermination of variability of terpenes and terpenoids in Cannabis sativa<\/em> by gas chromatography-flame ionization detection and gas chromatography-mass spectrometry\u201d.
Sol Giovannoni; Carlina Lancioni; Cristian Vaccarini; Daniela Sedan; Dario Andrinolo; Cecilia Castells
J. Chromatogr. A, 463669 (2023); doi<\/a>.<\/p>\n\n\n\n

“Modified lanthanide-doped carbon dots as a novel nanochemosensor for efficient detection of water in toluene and its potential application in lubricant base oils”
Christian Chimeno-Trinchet, Maria Emilia Pacheco, Alfonso Fern\u00e1ndez-Gonz\u00e1lez, Rosana Bad\u00eda-La\u00ed\u00f1o
Mikrochim Acta, (2023) doi<\/a><\/p>\n\n\n\n

“New europium-doped carbon nanoparticles showing long-lifetime photoluminescence: Synthesis, characterization and application to the determination of tetracycline in waters”
Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy, 284, (2023), 121756 doi<\/a><\/p>\n\n\n\n

A\u00d1O 2022<\/strong><\/p>\n\n\n\n

\u201cSolid-Phase Microextraction\u2014Gas Chromatography Analytical Strategies for Pesticide Analysis\u201d.
Juan Aspromonte; Carlina Lancioni; Giorgia Purcaro
Methods Protoc., 5<\/em>(5), 82 (2022); doi<\/a>.<\/p>\n\n\n\n

\u201cHeadspace Solid-Phase Microextraction: Fundamentals and Recent Advances\u201d.
Carlina Lancioni; Cecilia Castells; Roberto Candal; Marcos Tasc\u00f3n
Adv. Sci., 100035<\/em> (2022); doi<\/a>.<\/p>\n\n\n\n

\u201cDetermination of polycyclic aromatic hydrocarbons in surface waters by high performance liquid chromatography previous to preconcentration through solid-phase extraction by using polymeric monoliths\u201d.
Emilia Frickel Critto; Giselle Medina; Mario Reta; Agust\u00edn Acquaviva
J. Chromatogr. A, 463397 (2022); doi<\/a>.<\/p>\n\n\n\n

\u201cComprehensive two-dimensional liquid chromatographic method (Chiral\u202f\u00d7\u202fAchiral) for the simultaneous resolution of pesticides\u201d.
M. E. D\u00edaz Merino; A. Acquaviva; J. M. Padr\u00f3, C. B. Castells.
J. Chromatogr. A, 463126 (2022); doi<\/a>.<\/p>\n\n\n\n

A\u00d1O 2021<\/strong><\/p>\n\n\n\n

\u201cDevelopment of a green and efficient methodology for the heterocyclic aromatic amine determination in biomass samples generated from cigarette combustion and tobacco\u201d.
Romina Canales, Mar\u00eda Gui\u00f1ez, Carolina Talio, Mario Reta, Soledad Cerutti
Environ. Sci. Pollut. Res., 28, 5205\u20135217 (2021); doi<\/a>.<\/p>\n\n\n\n

\u201cDevelopment of a Background Electrolyte for the Determination of Inorganic Cations in High Ionic Strength Samples by Capillary Electrophoresis with Indirect UV-absorption Detection\u201d.
Carlina Lancioni, Juan M. Aspromonte, Marcos Tascon, Leonardo G. Gagliardi.
J. Chromatogr. A, 462091; 2021; doi<\/a>.<\/p>\n\n\n\n

A\u00d1O 2020<\/strong><\/p>\n\n\n\n

\u201cImproving separation optimization in capillary electrophoresis by using a general quality criterion”\u201d.
Roger Pero-Gascon, Marcos Tascon, Victoria Sanz-Nebot, Leonardo G. Gagliardi, Fernando Benavente.
Talanta 120399; 2020; doi<\/a>.<\/p>\n\n\n\n

\u201cPolymeric monolithic microcartridges with gold nanoparticles for the analysis of protein biomarkers by on-line solid-phase extraction capillary electrophoresis-mass spectrometry\u201d.
Laura Pont, Gemma Marina, Mar\u00eda Vergara-Barber\u00e1n, Leonardo G. Gagliardi, V Sanz-Nebot, J. M. Herrero-Mart\u00ednez, F. Benavente.
J. Chromatogr. A, 461097; 2020; doi<\/a>.<\/p>\n\n\n\n

\u201cMulti-response optimization of a green solid-phase extraction for the analysis of heterocyclic aromatic amines in environmental samples\u201d.
R. Canales, L. Mari\u00f1o Repizo, M. Reta.
Analytical Methods, 2020, 12,<\/strong> 1504 – 1513; 2020; doi<\/a>.<\/p>\n\n\n\n

\u201cDevelopment of monolithic sorbent cartridges (m-SPE) for the extraction of non-steroidal anti-inflammatory drugs from surface waters and their determination by HPLC\u201d.
G. S. Medina, A. Acquaviva, M. Reta.
Microchem. J., 159, 105447; 2020; doi<\/a>.<\/p>\n\n\n\n

\u201cDevelopment of a green and efficient methodology for the heterocyclic aromatic amine determination in biomass samples generated from cigarette combustion and tobacco\u201d.
R. Canales, M. Gui\u00f1ez, C. Talio, M. Reta, S. Cerutti.
Environ. Sci. Pollut. Res; 2020; doi<\/a>.<\/p>\n\n\n\n

\u201cStudy of enantioseparation of \u03b2-blockers using amylose tris<\/em>(3-chloro-5-methylphenylcarbamate) as chiral stationary phase under polar-organic, reversed-phase and hydrophilic interaction liquid chromatography conditions\u201d.
M. E. D\u00edaz Merino; C. Lancioni; J. M. Padr\u00f3, C. B. Castells.
J. Chromatogr. A; 2020 vol. 1634; doi<\/a>.<\/p>\n\n\n\n

\u201cChiral x achiral multidimensional liquid chromatography. Application to the enantioseparation of dintitrophenyl amino acids in honey samples and their fingerprint classification\u201d.
A. Acquaviva; G. Siano; P. Quintas; M. R. Filgueira; C. B. Castells.
J. Chromatogr. A; 2020 vol. 1614; doi<\/a>.<\/p>\n\n\n\n

\u201cChiral separation of several pesticides on an immobilized amylose tris(3-chloro-5-methylphenylcarbamate) column under polar-organic conditions. Influence of mobile phase and temperature on enantioselectivity\u201d.
M. E. D\u00edaz Merino; C. Lancioni; J. M. Padr\u00f3, C. B. Castells.
J. Chromatogr. A; 2020 vol. 1624; doi<\/a>.<\/p>\n\n\n\n

\u201cEfficiency of capillary GC columns based on phosphonium ionic liquids\u201d.
N. R. Ronco; C. Lancioni; L. M. Romero; C. B. Castells.
J. Chromatogr. A; 2020 vol. 162; doi<\/a>.<\/p>\n\n\n\n

A\u00d1O 2019<\/strong><\/p>\n\n\n\n

\u201cDetermination of Thermodynamic Binding Constants by Affinity Capillary Electrophoresis\u201d.
Carlina Lancioni, Sonia Kenchkarian, Leonardo G. Gagliardi.
Talanta 448\u2013454; 2019 ; doi<\/a>.<\/p>\n\n\n\n

\u201cOrganic monolithic capillary columns coated with cellulose tris(3,5-dimethylphenyl carbamate) for enantioseparations by capillary HPLC\u201d.
N. R Echevarr\u00eda; S. Keunchkarian; J. Villarroel Rocha; K. Sapag; M. Reta.
Microchem. J.; 2019 vol. 149; doi<\/a>.<\/p>\n\n\n\n

\u201cEnantioseparation of the racemates of a number of pesticides on a silica-based column with immobilized amylose tris(3-chloro-5-methylphenylcarbamate)\u201d.
M. E. D\u00edaz Merino; R. N. Echevarr\u00eda; E. Lubomirsky; J. M. Padr\u00f3; C. B. Castells.
Microchem. J.; 2019; doi<\/a>.<\/p>\n\n\n\n

\u201cDetermination of gas\u2013liquid partition coefficients of several organic solutes in trihexyl (tetradecyl) phosphonium dicyanamide using capillary gas chromatography columns\u201d.
N. R. Ronco; F. Menestrina; L. M. Romero; C. B. Castells.
J. Chromatogr. A; 2019 vol. 1584 p. 179 \u2013 186; doi<\/a>.<\/p>\n\n\n\n

\u201cDetermination of thermodynamic binding constants by affinity capillary electrophoresis\u201d.
C. Lancioni; S. Keunchkarian; C. B. Castells; L. G. Gagliardi.
Talanta; 2019 vol. 192 p. 448 \u2013 454; doi<\/a>.<\/p>\n\n\n\n

A\u00d1O 2018<\/strong><\/p>\n\n\n\n

\u201cPhotografted methacrylate-based monolithic columns coated with cellulose tris(3,5-dimethylphenylcarbamate) for chiral separation in CEC\u201d.
R. N Echevarr\u00eda; E. J. Carrasco Correa; S. Keunchkarian; M. Reta; J. M. Herrero-Mart\u00ednez.
J. Sep. Sci.; 2018; doi<\/a>.<\/p>\n\n\n\n

\u201cNarrow bore post column derivatisation assays via reaction flow chromatography\u201d.
A. Acquaviva; A. Jones; G. R. Dennis; C. B. Castells; R. A. Shalliker; A. Soliven.
Microchem. J.; 2018 vol. 142 p. 181 \u2013 186; doi<\/a>.<\/p>\n\n\n\n

\u201cEnantioseparation of polar pesticides on chiral capillary columns based on permethyl-\u03b2-cyclodextrin in matrices of different polarities\u201d.
F. Menestrina; N. R. Ronco; L. M. Romero; C. B. Castells.
Microchem. J; 2018 vol. 140 p. 52 \u2013 59; doi<\/a>.<\/p>\n\n\n\n

\u201cEnantiomeric separations by capillary electrophoresis: Theoretical method to determine optimum chiral selector concentration\u201d.
C. Lancioni: S. Keunchkarian; C. B. Castells; L. G. Gagliardi.
J. Chromatogr. A; 2018 vol. 1539 p. 71 \u2013 77; doi<\/a>.<\/p>\n\n\n\n

\u201cHigh throughput method to characterize acid-base properties of insoluble drug candidates in water\u201d.
D. Benito; A. Acquaviva; C. B. Castells; L. G. Gagliardi.
J. Pharmaceut Biomed; 2018 vol. 154 p. 404; doi<\/a>.<\/p>\n\n\n\n

A\u00d1O 2017<\/strong><\/p>\n\n\n\n

\u201cA rapid and simple method for the determination of psychoactive alkaloids by CE-UV. Application to Peganum harmala seeds infusions\u201d.
Marcos Tasc\u00f3n, Fernando J. Benavente, Nora M. Vizioli, Leonardo G. Gagliardi.
Drug Test. Anal. 596-602; 2017; doi<\/a>.<\/p>\n\n\n\n

\u201cParts-per-trillion detection of harmala alkaloids in Undaria pinnatifida algae by on-line solid phase extraction capillary electrophoresis mass spectrometry\u201d.
Marcos Tascon, Leonardo G. Gagliardi, Fernando Benavente.
Anal. Chim. Acta 60-67; 2017; doi<\/a>.<\/p>\n\n\n\n

\u201cDetermining heterocyclic aromatic amines in aqueous samples: a novel dispersive liquid-liquid micro-extraction method based on the solidification of the floating organic drop and ultrasound assisted back extraction followed by UPLC-MS\/MS\u201d.
R. Canales, M. E. Gui\u00f1ez, C. Baz\u00e1n, M. Reta, S. Cerutti.
Talanta, 174, 548\u2013555; 2017; doi<\/a>.<\/p>\n\n\n\n

\u201cChiral separation of aryloxyphenoxy-propionate herbicides in a permethyl-\u03b2-cyclodextrin based column. Influence of temperature and mobile phase composition on enantioselectivity\u201d.
E. Lubomirsky; H. Di Loreto; J. M. Padr\u00f3; C. B. Castells.
Electrophoresis; 2017; doi<\/a>.<\/p>\n\n\n\n

\u201cDetermination of gas-liquid partition coefficients of several organic solutes in trihexyl(tetradecyl)phosphonium bromide using capillary GC columns\u201d.
N. R. Ronco, F. Menestrina, L. M. Romero, C. B. Castells.
J. Chromatogr. A; 2017; doi<\/a>.<\/p>\n\n\n\n

“Mn-doped ZnS phosphorescent quantum dots: Coumarins optical sensors\u201d.
M. E. Pacheco, C. B. Castells, L. Bruzzone.
Sensor Actuat B-Chem.; 2017 vol. 238 p. 660 \u2013 666; doi<\/a>.<\/p>\n\n\n\n

A\u00d1O 2016<\/strong><\/p>\n\n\n\n

\u201cQuality Criterion to Optimize Separations in Capillary Electrophoresis.: Application to the Analysis of Harmala Alkaloids\u201d.
Marcos Tasc\u00f3n, Fernando J. Benavente, Cecilia B. Castells, Leonardo G. Gagliardi. J. Chromatogr. A. 190-196; 2016; doi<\/a>.<\/p>\n\n\n\n

\u201cSolvatochromic parameters of imidazolium-, hydroxyammonium-, pyridinium- andphosphonium-based roomtemperature ionic liquids\u201d.
J. M. Padr\u00f3, M. Reta.
J. Molec. Liq., 213, 107-114; 2016; doi<\/a>.<\/p>\n\n\n\n

\u201cDevelopment of a dispersive liquid-liquid microextraction technique for the analysis of aryloxyphenoxy-propionate herbicides in soy-based foods\u201d.
E. Lubomirsky, J. M. Padr\u00f3, M. Reta.
Microchem. J., 129, 63-70; 2016; doi<\/a>.<\/p>\n\n\n\n

\u201cDevelopment of a dispersive liquid\u2013liquid microextraction method using a lighter than water ionic liquid for the analysis of polycyclic aromatic hydrocarbons in water samples\u201d.
G. Medina, M. Reta.
J. Sep. Sci., 39, 4209-4218; 2016; doi<\/a>.<\/p>\n\n\n\n

\u201cAnalysis of citrulline and metabolic related amino acids in plasma by derivatization and RPLC. Application of the extrapolative internal standard calibration method\u201d.
A. Acquaviva; L. M. Romero; C. B. Castells.
Microchem. J.; 2016 vol. 129 p. 29 \u2013 35; doi<\/a>.<\/p>\n\n\n\n

\u201cEnantiomeric analysis of overlapped chromatographic profiles with presence of interferences. Application to the enantiomeric composition determination of ibuprofen in a pharmaceutical formulation containing homatropine\u201d.
J. M. Padr\u00f3; J. Osorio Grisales; J. Arancibia; A. Olivieri; C. B. Castells; C. B. Castells.
J. Chromatogr. A; 2016 vol. 1467 p. 255 \u2013 260; doi<\/a>.<\/p>\n\n\n\n

\u201cChiral ligand-exchange chromatography with Cinchona alkaloids. Exploring experimental conditions for enantioseparation of \u03b1-amino acids\u201d.
R. N. Echevarr\u00eda; C. A. Franca; M. Tasc\u00f3n; C. B. Castells; S. Keunchkarian.
Microchem. J.; 2016 vol. 129 p. 104 \u2013 110; doi<\/a>.<\/p>\n\n\n\n

\u201cEnantioselective gas chromatography with functionalized cyclodextrins as chiral selectors. Fundamentals of the measurement of absolute association constants using capillary columns\u201d.
F. Menestrina; N. Ronco; C. B Castells.
J. Chromatogr. A; 2016 vol. 1467 p. 482 \u2013 489; doi<\/a>.<\/p>\n\n\n\n

\u201cChiral analysis of derivatized amino acids from kefir by gas chromatography\u201d.
F. Menestrina; J. Osorio Grisales; C. B. Castells.
Microchem. J; 2016 vol. 128 p. 267 \u2013 273; doi<\/a>.<\/p>\n\n\n\n

\u201cA new quality criterion to optimize separations in capillary electrophoresis. Application to the analysis of harmala alkaloids\u201d.
M. Tasc\u00f3n; F. Benavente; C. B. Castells; L. G. Gagliardi.
J. Chromatogr. A; 2016 vol. 1490 p. 190 \u2013 196; doi<\/a>.<\/p>\n\n\n\n

A\u00d1O 2015<\/strong><\/p>\n\n\n\n

\u201cScope of partial least-squares regression applied to the enantiomeric composition determination of ketoprofen from strongly overlapped chromatographic profiles\u201d.
J. M. Padr\u00f3; J. Osorio Grisales; J. Arancibia; A. C. Olivieri; C. B. Castells; C. B. Castells.
J. Sep. Sci.; 2015 p. 2423 \u2013 2430; doi<\/a>.<\/p>\n\n\n\n

\u201cFast determination of harmala alkaloids in edible algae by capillary electrophoresis mass spectrometry\u201d.
M. Tasc\u00f3n; F. Benavente; V. M. Sanz-Nebot; L. G. Gagliardi.
Anal. & Bioanal. Chem; doi<\/a>.<\/p>\n\n\n\n

\u201cA high performance system to study the influence of temperature in on-line solid-phase extraction capillary electrophoresis\u201d.
M. Tasc\u00f3n; F. Benavente; V. M. Sanz-Nebot; L. G. Gagliardi.
Anal. Chim. Acta; 863 (2015)78-85; doi<\/a>.<\/p>\n\n\n\n

\u201cDevelopment of an ionic liquid based-dispersive liquid-liquid microextraction method for the determination of antichagasic drugs in human breast milk. Optimization by central composite design\u201d.
J.M. Padr\u00f3; R. Pellegrino Vidal; R. N. Echevarr\u00eda; A. Califano; M. Reta.
J. Sep. Sci.; doi<\/a>.<\/p>\n\n\n\n

A\u00d1O 2014<\/strong><\/p>\n\n\n\n

\u201cNovel magnetite nanoparticles coated with waste sourced bio-based substances as sustainable and renewable adsorbing materials\u201d.
Giuliana Magnacca, Alex Allera, Enzo Montoneri, Luisella Celi, Dami\u00e1n E. Benito, Leonardo G. Gagliardi, M\u00f3nica C. Gonzalez, Daniel O. M\u00e1rtire, Luciano Carlos.
ACS Sustainable Chem. Eng. 1518-1524; doi<\/a>.<\/p>\n\n\n\n

\u201cReliable and simple analytical methods for determination of citrulline and metabolically related amino acids by liquid chromatography after derivatization: Comparison between monolithic and core-shell columns\u201d.
A. Acquaviva; L. M. Romero; C. B. Castells; G. Ramis-Ramos; J. M. Herrero-Mart\u00ednez.
Anal. Methods; 6(2014) 5830-5837; doi<\/a>.<\/p>\n\n\n\n

\u201cNew Method to Sinterize Silica Frits to Produce Capillary Microcolumns\u201d.
S. Keunchkarian; P. J. Lebed; B. Sliz; C. B. Castells; L. G. Gagliardi.
Anal. Chim. Acta; 820(2014)168-175; doi<\/a>.<\/p>\n\n\n\n

\u201cDetermination of citrulline and the prominent amino acids involved in small intestine diseases by liquid chromatography after derivatization. Comparison of separation by a monolithic and a core-shell column\u201d.
A. Acquaviva; L. M. Romero; C. Castells; G. Ramis-Ramos; J. M. Herrero-Mart\u00ednez.
Anal. Methods; 6(2014)5830-5837.<\/p>\n\n\n\n

\u201cMeasurements of association constants between enantiomers and chiral selectors by capillary gas chromatography. Theoretical and practical considerations\u201d.
P. J. Lebed; S. Keunchkarian; J. Osorio Grisales; C. B. Castells.
J. Chromatogr. A ; 1324(2014)198-206; doi<\/a>.<\/p>\n\n\n\n

\u201cAutomatized sspKa measurements of dihydrogen phosphate and Tris(hydroxymethyl) aminomethane in acetonitrile\/water mixtures from 20 to 60 \u00b0C”.
A. Acquaviva; M. Tasc\u00f3n; J. M. Padr\u00f3, L. G. Gagliardi.
Talanta; 127(2014)196-203; doi<\/a>.<\/p>\n\n\n\n

\u201cPartition coefficients of organic compounds between water and imidazolium-, pyridinium-, and phosphonium-based ionic liquids\u201d.
J. M. Padr\u00f3; R. Pellegrino Vidal; M. Reta.
Anal. & Bioanal. Chem.; 406(2014)8021-8031; doi<\/a>.<\/p>\n\n\n\n

\u201cEffect of temperature and solvent composition on acid dissociation equilibria, II: Automatized measurements of dihydrogen phosphate and tris(hydroxymethyl) aminomethane in acetonitrile\/water mixtures and from 20 to 60 \u00baC\u201d.
A. Acquaviva; M. Tascon; J. M. Padr\u00f3; L. G. Gagliardi; C. B. Castells.
Talanta, 127, 196-203.<\/p>\n\n\n\n

A\u00d1O 2013<\/strong><\/p>\n\n\n\n

\u201cEnantioseparation of a-amino acids by means of Cinchona alkaloids as selectors in chiral ligand exchange chromatography\u201d.
S. Keunchkarian; C. A. Franca; L. G. Gagliardi; C. B. Castells.
J. Chromatogr. A; 2013, 1298, 103-108; doi<\/a>.<\/p>\n\n\n\n

\u201cA simple and efficient HPLC method for benznidazole dosage in human breast milk\u201d.
M. E. Mars\u00f3n; J. M. Padr\u00f3; M. Reta; J. Altcheh, F. Garc\u00eda-Bournissen, G. E. Mastrantonio.
TDM; 2013, 35, 522-526; doi<\/a>.<\/p>\n\n\n\n

\u201cAccurate method for gas-liquid partition coefficient determinations using capillary gas chromatography. Alkanols in squalane\u201d.
M. Tasc\u00f3n; L. M. Romero; A. Acquaviva, C. B. Castells.
J. Chromatogr. A; 2013, 1294, 130-136; doi<\/a>.<\/p>\n\n\n\n

\u201cDevelopment of an ionic liquid based dispersive liquid-liquid microextraction method for the analysis of nifurtimox and benznidazole in human plasma\u201d.
J. M. Padr\u00f3; M. E. Mars\u00f3n; G. E. Mastrantonio; J. Altcheh; F. Garc\u00eda-Bournissen; M. Reta.
Talanta; 107(2013)95-102; doi<\/a>.<\/p>\n\n\n\n

\u201cMajor phenolics in yerba mate extracts (Ilex paraguariensis) and their contribution to the total antioxidant capacity\u201d.
L. Deladino; A. Schneider Teixeira; M. Reta; A. D. Molina Garc\u00eda; A. S. Navarro; M. N. Martino.
Food & Nutrition Sci.; 4(2013) 8A, 154-162.; doi<\/a>.<\/p>\n\n\n\n

\u201cNew method for the analysis of non-polar heterocyclic aromatic amines in beefburguers by using microwave-assisted extraction and dispersive liquid-ionic liquid microextraction\u201d.
L. B. Agudelo Mesa; J. M. Padr\u00f3; M. Reta.
Food Chemistry; 2013, 141, 1694-1701; doi<\/a>.<\/p>\n\n\n\n

A\u00d1O 2012<\/strong><\/p>\n\n\n\n

\u201cDevelopment of a chiral stationary phase based on cinchonidine. Comparison with a quinine-based chiral column\u201d.
S. Keunchkarian; J. Osorio Grisales; J. M. Padr\u00f3; S. Boeris, C. B. Castells.
Chirality; 2012, 24, 512-518; doi<\/a>.<\/p>\n\n\n\n

\u201cEffect of temperature and solvent composition on acid dissociation equilibria. I. Sequenced pKa(s,s) determination of compounds commonly used as buffers in HPLC coupled to MS detection\u201d.
J. M. Padr\u00f3; A. Acquaviva; M. Tascon; L. G. Gagliardi; C. B. Castells.
Anal. Chim. Acta; 2012, 725, 87-94; doi<\/a>.<\/p>\n\n\n\n

\u201cPredicting retention in reversed-phase liquid chromatography at different mobile phase compositions and temperatures by using the solvation parameter model\u201d.
J. Gotta; S. Keunchkarian; C. B. Castells; M. Reta.
J. Sep. Sci.; 2012, 35, 2699-2709; doi<\/a>.<\/p>\n\n\n\n

\u201cDetermination of enantiomeric composition of ibuprofen in pharmaceutical formulations by partial least-squares regression of strongly overlapped chromatographic profiles\u201d.
J. Osorio Grisales; J. A. Arancibia; C. B. Castells; A. C. Olivieri.
J. Chromatogr. B; 2012; 910, 78-83; doi<\/a>.<\/p>\n\n\n\n

\u201cA simple, robust orthogonal background correction method for two-dimensional liquid chromatography\u201d.
M. R. Filgueira; C. B. Castells; P.W. Carr.
Anal. Chem.; 2012, 84, 6747-6752; doi<\/a>.<\/p>\n\n\n\n

“Polyphenol input to the antioxidant activity of yerba mate (Ilex paraguariensis) extracts\u201d.
J. Valerga; M. Reta; M.C. Lanari.
LWT-Food Sci. & Technol.; 2012, 45, 28-35; doi<\/a>.<\/p>\n\n\n\n

A\u00d1O 2011<\/strong><\/p>\n\n\n\n

\u201cRapid and sensitive gradient liquid chromatography method for the quantitation of intracellular 2-hydroxyethidium ion\u201d.
P. J. Lebed; J. Osorio Grisales; S. Keunchkarian; J. Gotta; M. Giambelluca; C. B. Castells.
Anal. Methods; 2011, 3, 593-598; doi<\/a>.<\/p>\n\n\n\n

\u201cSimultaneous effect of pH, temperature and mobile phase composition in the chromatographic retention of ionizable compounds\u201d.
P. Agrafiotou; C. R\u00e0fols; C. B. Castells; E. Bosch; M. Ros\u00e9s.
J. Chromatogr. A; 2011; 1218, 4995-5009; doi<\/a>.<\/p>\n\n\n\n

\u201cSynthesis and evaluation of a chiral stationary phase based on quinine. Enantioresolution of dinitrophenyl derivatives of a-amino acids\u201d.
S. Keunchkarian; J. M. Padr\u00f3; J. Gotta; A. M. Nardillo; C. B. Castells.
J. Chromatogr. A; 2011,1218, 3660-3668; doi<\/a>.<\/p>\n\n\n\n

\u201cImproving Peak Capacity in Fast On-Line Comprehensive TwoDimensional Liquid Chromatography by Post First Dimension Flow-Splitting\u201d.
M. R. Filgueira; Y. Huang; K. Witt; C. B. Castells; P. W. Carr.
Anal. Chem.; 2011, 83, 9531-9539; doi<\/a>.<\/p>\n\n\n\n

\u201cThe antimutagenic capacity of the aqueiious extract of Baccharis articulate (Lam.) Persoon\u201d.
M. Rodriguez; L. Gianuzzi; M. Reta; M. L. Larramendy.
Toxicological and Environmental Chemistry; 2011, 93, 251-260; doi<\/a>.<\/p>\n\n\n\n

\u201cPredicting the partitioning of biological compounds between room-temperature ionic liquids and water by means of the Solvation Parameter Model\u201d.
J. M. Padr\u00f3; A. Ponzinibbio; L. B. Agudelo Mesa; M. Reta.
Anal. & Bioanal. Chem.; 2011, 399, 2807-2820; doi<\/a>.<\/p>\n\n\n\n

A\u00d1O 2010<\/strong><\/p>\n\n\n\n

\u201cFast RPLC analysis of pharmaceutical compounds at moderately elevated temperatures by using a conventional instrument. Comparison between particulated and monolithic columns\u201d.
J. Gotta; J. Osorio Grisales; M. Reta; C. B. Castells.
J. Sep. Sci.; 2010, 33, 2645-2653; doi<\/a>.<\/p>\n\n\n\n

\u201cComparison between phase transfer and cloud point methodologies for the micellar extraction of biogenic amines\u201d.
L. M. Romero; J. Osorio Grisales; M. Reta.
Talanta; 2010, 81, 1431-1437; doi<\/a>.<\/p>\n\n\n\n

\u201cBinding of several benzodiazepines to bovine serum albumin: Fluorescence study\u201d.
R. G. Machicote, M. E. Pacheco, L. Bruzzone.
SAA; 2010, 77, 466-472; doi<\/a>.<\/p>\n\n\n\n

\u201cDissociation constants and thermodynamic ionization quantities of o-phthalic acid in acetonitrile\/water mixtures. Evaluation of the potassium hydrogen phthalate solutions as pH reference standard\u201d.
L. G. Gagliardi; C. B. Castells; M. Ros\u00e9s; C. R\u00e0fols; E. Bosch.
J. Chem. Eng. Data; 2010, 55, 85-91; doi<\/a>.<\/p>\n\n\n\n

TESIS DOCTORALES<\/strong><\/p>\n\n\n\n

T\u00edtulo:<\/strong> “Desarrollo de columnas capilares con l\u00edquidos i\u00f3nicos como fases estacionarias para cromatograf\u00eda de gases. Aplicaci\u00f3n a la separaci\u00f3n de contaminantes ambientales”
Autor:<\/strong> Nicol\u00e1s R. Ronco (2020)
Descargar<\/a><\/strong><\/p>\n\n\n\n

T\u00edtulo:<\/strong> “Desarrollo de sistemas para la electroseparaci\u00f3n enantiom\u00e9rica de compuestos quirales”
Autor:<\/strong> Carlina Lancioni (2019)
Descargar<\/a><\/strong><\/p>\n\n\n\n

T\u00edtulo:<\/strong> “Desarrollo de columnas monol\u00edticas quirales para HPLC capilar. Aplicaci\u00f3n a la determinaci\u00f3n de contaminantes emergentes”
Autor:<\/strong> Ester Lubomirsky (2019)
Descargar<\/a><\/strong><\/p>\n\n\n\n

T\u00edtulo:<\/strong> “Desarrollo de m\u00e9todos de extracci\u00f3n empleando l\u00edquidos i\u00f3nicos y pol\u00edmeros monol\u00edticos para la determinaci\u00f3n de contaminantes ambientales en agua de r\u00edo.”
Autor:<\/strong> Giselle Medina (2019)
Descargar<\/a><\/strong><\/p>\n\n\n\n

T\u00edtulo:<\/strong> “Desarrollo de columnas capilares monol\u00edticas quirales para t\u00e9cnicas separativas miniaturizadas. Aplicaci\u00f3n a la enantioseparaci\u00f3n de compuestos de inter\u00e9s biol\u00f3gico”
Autor:<\/strong> Romina Echevarr\u00eda (2018)
Descargar<\/a><\/strong><\/p>\n\n\n\n

T\u00edtulo:<\/strong> “Desarrollo de columnas capilares quirales para su empleo en cromatograf\u00eda de gases: aplicaci\u00f3n a la separaci\u00f3n de contaminantes ambientales quirales”
Autor:<\/strong> Fiorella Menestrina (2018)
Descargar<\/a><\/strong><\/p>\n\n\n\n

T\u00edtulo:<\/strong> “Desarrollo de sensores fosforescentes en estado l\u00edquido a temperatura ambiente”
Autor:<\/strong> Mar\u00eda Emilia Pacheco (2017)
Descargar<\/a><\/strong><\/p>\n\n\n\n

T\u00edtulo:<\/strong> “Desarrollo de sistemas de preconcentraci\u00f3n “on-line” para an\u00e1lisis de muestras de inter\u00e9s biol\u00f3gico mediante electroforesis capilar”
Autor:<\/strong> Marcos Tasc\u00f3n (2015)
Descargar<\/a><\/strong><\/p>\n\n\n\n

T\u00edtulo:<\/strong> “Determinaci\u00f3n de aminas arom\u00e1ticas heteroc\u00edclicas en carnes cocidas mediante extracci\u00f3n con microondas y l\u00edquidos i\u00f3nicos”
Autor:<\/strong> Leidy Bibiana, Agudelo Mesa (2015)
Descargar<\/a><\/strong><\/p>\n\n\n\n

T\u00edtulo:<\/strong> “Desarrollo y optimizaci\u00f3n de metodolog\u00edas separativas de an\u00e1lisis de citrulina y amino\u00e1cidos metab\u00f3licamente relacionados”
Autor:<\/strong> Agust\u00edn Acquaviva (2014)
Descargar<\/a><\/strong><\/p>\n\n\n\n

T\u00edtulo:<\/strong> “Coeficientes de Partici\u00f3n entre l\u00edquidos i\u00f3nicos y agua. Aplicaci\u00f3n a la microextracci\u00f3n dispersiva de compuestos antichag\u00e1sicos en muestras biol\u00f3gicas”
Autor:<\/strong> Juan Manuel Padr\u00f3 (2014)
Descargar<\/a><\/strong><\/p>\n\n\n\n

T\u00edtulo:<\/strong> “Empleo de pol\u00edmeros impresos nanoestructurados en el desarrollo de optosensores”
Autor:<\/strong> Roberta Grisel Machicote (2014)
Descargar<\/a><\/strong><\/p>\n\n\n\n

<\/p>\n\n\n\n

TESINAS DE GRADO<\/strong><\/p>\n\n\n\n

T\u00edtulo:<\/strong> “Predicci\u00f3n de la retenci\u00f3n y separaci\u00f3n de agroqu\u00edmicos en cromatograf\u00eda de l\u00edquidos en fase inversa en funci\u00f3n de composici\u00f3n de fase m\u00f3vil, pH y temperatura de la columna”
Autor:<\/strong> Pedro N. Cifuentes (2022)
Des<\/a>cargar<\/a><\/strong><\/p>\n\n\n\n

T\u00edtulo:<\/strong> “Desarrollo de dispositivos nanotecnol\u00f3gicos para la retenci\u00f3n, remoci\u00f3n
y control anal\u00edtico de ars\u00e9nico en aguas para consumo humano”
Autor:<\/strong> Bel\u00e9n M. Cingolani (2022)
Des<\/a>cargar<\/a><\/strong><\/p>\n\n\n\n

T\u00edtulo:<\/strong> ” “
Autor:<\/strong> Emilce Rodriguez (2022)
Des<\/a>cargar<\/a><\/strong><\/p>\n\n\n\n

T\u00edtulo:<\/strong> “M\u00e9todos de separaci\u00f3n de enanti\u00f3meros: desarrollo, evoluci\u00f3n y aplicaciones de columnas quirales para cromatograf\u00eda de l\u00edquidos y de gases.”
Autor:<\/strong> Daiana L. Prince (2021)
Descargar<\/a><\/strong><\/p>\n\n\n\n

T\u00edtulo:<\/strong> “Estrategias de optimizaci\u00f3n de variables en separaciones por cromatograf\u00eda de l\u00edquidos de alta resoluci\u00f3n.”
Autor:<\/strong> Sebasti\u00e1n Javier Caruso (2021)
Descargar<\/a><\/strong><\/p>\n\n\n\n

T\u00edtulo: <\/strong>“Desarrollo de m\u00e9todos de an\u00e1lisis de terpenos y compuestos terpenoides por cromatograf\u00eda. Comparaci\u00f3n cr\u00edtica de resultados obtenidos mediante CG y HPLC.”
Autor:<\/strong> Sol Giovannoni (2021)
Descargar<\/a><\/strong><\/p>\n\n\n\n

T\u00edtulo:<\/strong> “M\u00e9todos de an\u00e1lisis de hidrocarburos arom\u00e1ticos polic\u00edclicos (HAPS) como contaminantes prioritarios en aguas por cromatograf\u00eda de l\u00edquidos y t\u00e9cnicas de preconcetraci\u00f3n”
Autor:<\/strong> Emilia Josefina Frickel Critto (2020)
Descargar<\/a><\/strong><\/p>\n\n\n\n

T\u00edtulo:<\/strong> “Estudio Potenciom\u00e9trico de Equilibrios de Disociaci\u00f3n \u00c1cido-Base en Mezclas de Solventes Polares”
Autor:<\/strong> Dami\u00e1n Ezequiel Benito (2017)
Descargar<\/a><\/strong><\/p>\n\n\n\n

T\u00edtulo:<\/strong> “Desarrollo de m\u00e9todos para la derivatizaci\u00f3n y cuantificaci\u00f3n de glufosinato, glifosato y \u00e1cido aminometilfosf\u00f3nico”
Autor:<\/strong> Brenda Bel\u00e9n Sliz (2017)
Descargar<\/a><\/strong><\/p>\n","protected":false},"excerpt":{"rendered":"

En nuestro laboratorio mantenemos y promovemos un fuerte compromiso con la investigaci\u00f3n y el desarrollo de metodolog\u00edas y tecnolog\u00edas de an\u00e1lisis espec\u00edficas para distintos tipos de muestras y matrices que mejoren el rendimiento de los m\u00e9todos anal\u00edticos vigentes, materializ\u00e1ndose en los numerosos trabajos cient\u00edficos publicados por los integrantes del laboratorio en revistas de alto impactoContinue reading “Publicaciones, Tesis y Tesinas”<\/span><\/a><\/p>\n","protected":false},"author":2,"featured_media":0,"parent":0,"menu_order":0,"comment_status":"closed","ping_status":"closed","template":"","meta":{"footnotes":""},"class_list":["post-54","page","type-page","status-publish","hentry","entry"],"_links":{"self":[{"href":"https:\/\/lidma.exactas.unlp.edu.ar\/index.php\/wp-json\/wp\/v2\/pages\/54","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/lidma.exactas.unlp.edu.ar\/index.php\/wp-json\/wp\/v2\/pages"}],"about":[{"href":"https:\/\/lidma.exactas.unlp.edu.ar\/index.php\/wp-json\/wp\/v2\/types\/page"}],"author":[{"embeddable":true,"href":"https:\/\/lidma.exactas.unlp.edu.ar\/index.php\/wp-json\/wp\/v2\/users\/2"}],"replies":[{"embeddable":true,"href":"https:\/\/lidma.exactas.unlp.edu.ar\/index.php\/wp-json\/wp\/v2\/comments?post=54"}],"version-history":[{"count":45,"href":"https:\/\/lidma.exactas.unlp.edu.ar\/index.php\/wp-json\/wp\/v2\/pages\/54\/revisions"}],"predecessor-version":[{"id":1087,"href":"https:\/\/lidma.exactas.unlp.edu.ar\/index.php\/wp-json\/wp\/v2\/pages\/54\/revisions\/1087"}],"wp:attachment":[{"href":"https:\/\/lidma.exactas.unlp.edu.ar\/index.php\/wp-json\/wp\/v2\/media?parent=54"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}